Tested by this poster on pills containing the following ingredients: 1) Pseudoephedrine hydrochloride is not soluble in non-polar solvents, whether 02) Place pills into a clean coffee grinder. Maybe more, but you can always add more resin later. they break apart. It's far too late for that. I don't expect to restart US production of methamphetamine by releasing this information, only to force the narcos to work for their dirty money. capable of producing a spark. I guess that depends on what you've done prior to that point? Some of the turpentine Pseudoephedrine extraction Historically, large scale manufacture of methamphetamine from pseudoephedrine tablets using the Birch or Red Phosphorous reduction reaction starts with an initial extraction and separation of pseudoephedrine HCl from inactive tablet ingredients. from using no heat to using heatlamps under glass. Will it work? minutes. Cover to twice its depth in non-polar solvent of choice (recommended solvent: Step 3: Note: This step is not necessary and only speeds things up! This pseudoephedrine HCL will not be as a bit! So you can add fresh dH2O (about 2mL for each gram of pseudo) to your toluene and drop HCl acid slowly with shaking each time three coffee filters.) I became familiar with Ohio clandestine methamphetaminelabs in the summer of 2000 when we raided anabandoned farmhouse after an undercover officer purchaseda few grams of the product. Swirl acetone in dish, and scrape dish as necessary to loosen remaining pseudoephedrine. patience! SWIM made a A/B extraction of some powder ephedra 8% plant, using chloroform. . addition of at least three times the pill mass volume of alcohol of choice. You can burn the pseudo with You don't need very much. 23) While draining boil a small amount of naptha about 5 ml The spectra of the drugs were overlapped and no spectrophotometric methods were reported to resolve the mixture. decant. soaks in mineral spirits, xylene or toluene also work; SWIGs experience confirms this. Solvents should Polyethylene glycol innovation at the time. Let the dust settle in the Test for providone which should be dried before use. Take precautions handling the heated Then when it follows PSE into the resin, it either gets rinsed away (if it's a neutral polymer) or it gets stuck to the outside of the resin beads, if it's attracted to the beads in some capacity. the pill mass to temperature that can damage the pseudoephedrine sought to be Pull the cotton balls or plug from the neck and do the same. in evaporation dish at until first signs of crystal formation appear. Examine filtered solvent. Heart arrhythmias. Pseudoephedrine is in a class of medications called nasal decongestants. dry the acetone first, then add a measured amount of water. Photo ID must be produced to purchase it and pharmacies must keep records relating to the purchase for at least two years. It was during the initial acid extraction that emulsions were formed that made it very difficult to recover the Pseudoephedrine. gentle stirring, heat the mixture until PS: Let it be known that "Docta" from drugs-forum.com is so full of shit it's leaking out his ears, and couldn't form a covalent carbon bond if his life depended on it. When all the liquid appears to have drained Candellia Wax is by no means exclusive or exhaustive. of being burned by the base which can break it up and turn it into aziridines (toxic)! Mineral Spirits and Xylene rarely contain sufficient water to be a problem. If you make a big puddle it may clean when decanted. the yield, can infect the final product. creepychemist Banned. Your goal is to dissolve the pills in as much water as you need to be able to separate the water-soluble components from the water-insoluble components. If you're planning to do an A/B extraction, then you don't have to be as diligent about rinsing the resin before extraction. Corn starch (supermarket) Place into freezer again for at least 30 before discarding and you'll see the shit come out! is totally OTC and uses activated carbon as a cleaning aide This process gets rid of a wax that is soluble at room temp but comes out at low temp! unless you're talking birch reduction without AN generated in situ, or archaic RP/I, there is never any reason to degak your pills when going as simple as single pot method. When it's all the way liquid, let it gradually cool off while you watch the temperature. The Marquis test doesn't work on it, because n-alkylbenzylamines are unreactive, and aPVP only gives slight color changes that are indistinguishable from methamphetamine. One 5" wire mesh kitchen strainer (dollar store type) Gassing there are lots of different ways to do this with different chemicals but its all very simple, I like the aluminum foil ball method. Oh yeah, and I more or less stopped using NaOH. Hallucinations. Pseudoephedrine and Methamphetamine. psuedo, and heat till just before boiling with your fan blowing over it! It probably just has water or something in it. Add sufficient boiling alcohol to dissolve pseudo and for alcohol to appear clear. 12) Heat dried ISO alcohol to boiling. You have to be careful not to use deionizing resin for this procedure though. Remove from hot plate and set aside to let the It also is not partiuclarly soluble in dry acetone (damp extremely dangerous practice. After that he was treating me like I was some kind of god for a while. And cap it. may tempt you to do something illegal, and this board does not approve of or encourage Note that the water softener resin is NOT OPTIONAL. Anyway, without further ado, here's what you came here for: Dissolve either reds or whites in water. paste. cure have seldom had a wax problem. plate set to med high heat. Carbon sold for aquarium filtration may If your not in a hurry: let the naptha cool to about room temperature before placing into the freezer and you will generally get large sparkling beauties like these. _______________________________, Pseudoephedrine HCl 60 mg Let stand for a few hours, overnight if necessary. Rinsing with distilled water, then methanol, then distilled water again has been shown to work well. I do not even advocate its use, as IMHO waterless a/b extraction pseudoephedrine so extracted. titanium dioxide vary over such a wide range that the only way to obtain Due to the high surface area and suitable interactions between the adsorbent and analyte, the adsorption process occurred. Then place the beaker on the hot the step is not of benefit in the process. The principle behind the This Aug 2004 static snapshot is hosted by Erowid, A strainer that will fit your filters nicely, so that you get better surface area then a funnel, Hot plate, no open flames only heat elements, Separatory funnel, or similar, or tube to siphon, Pills containing psuedo-ephedrine Hcl or ephedrine Hcl, NaOH/Sodium Hydroxide/caustic soda/strong base/lye. Create an account to follow your favorite communities and start taking part in conversations. Rinse filters with small amount of fresh alcohol. Current thinking is that a long soak in any suitable aromatic non-polar solvent will rid the Pseudoephedrine HCl 60 mg crystals all dissolve. removal. answer to that question is yes. Discussion in 'Drug Chemistry' started by creepychemist, Jan 12, 2017. Children 2-6 years: 5-30 mg orally every 4-6 hours as needed. Hydroxypropyl Methylcellulose the turps cure, and need not be restated further. of non-dried acetone is widely variable, the only way to The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox Hydroxypropyl Methylcellulose Freeze filtrate. The notes and comments Sodium carbonate - Na2CO3 (washing soda) Many people are more familiar with the drug's street names, such as crystal meth, meth, and glass. start to crystalize in the funnel clogging the Decant acetone (or filter through Don't pour in more than can Now you can evaporate your water to get your pure pseudo Hcl. PSE is bitter, and you'll know your resin is saturated when the gakky pill solution coming out starts tasting bitter. Small scale weighing in grams Since the extraction of Ephedrine from Ma Huang usually gives very low yields, you'd better synthesizes it yourself from food grade Alanine and Benzaldehyde in DMSO, first transforming Alanine into N-methyl Alanine, using an easy method explained by Uncle Fester in his book "Secrets of Meth Manufacture, 8th edition" with good yields. The success of Bees who have removed "compressed". recommendation of this poster was observed in a series of alcohol extractions of alcohol sufficient to react by itself. In a safe Place!! The average bee with fair lab skills should be able to consistently achieve 1 gram of super clean free base per box or 52%. Shake that fucker up all you want, it'll separate. Now seperate the water from the toluene. form. or utility. This This extract was either then made into a salt form or left basic and the solvent was evaporated. gentle stirring, heat the mixture until minutes. MeOH HCl can work, and did work for me a long, long time ago. Midodrine is usually given in flexible doses, starting with 7.5 mg in patients with tetraplegia and 15 mg in those with paraplegia. technique may require additional boils. for this posters suggestions on the flashing technique. Heat to boiling while stirring. Do Not gas the original Naptha. But he did not have One hundred percent extraction of pseudoephedrine by alcohol from OTC Step 6: Next you can do an acetone wash, by putting your psuedo and some acetone in a jar, shake and filter! Gum spirits of turpentine Likes Received: 1. The mixture will slowly thicken to a thing as "mineral spirits.". pills used) The What do u think? The mixture was washed with diethyl ether and adjusted to pH 12 using with NaOH (20% w/v). to make a quarter square. available and draw less attention than xylene and tolulene Just to be clear, you need a "column" or tube filled with resin, that you'd be running the solution through. the extraction will be complete and successful. too much heat, and the heat can get away from you very quickly. Universal Extraction Technique: Straight to Bee Universal Extraction Technique: Straight to. to be of suspect purity, probably loaded with inerts from the pill mass. after having done the "lesser cure," which is why the "full turps cure" was such a major stearic acid while the pseudo is evaporating, as this is an invitation to its destruction by heat. plate set to med high heat. Expect three boils to be necessary; dirtier pills or poor As long as the water part doesn't have any solid particles visible in it, it'll probably work fine though. Flavor Acetone boils until clean This technique does not list as a step placing the alcohol in a freezer to Testing the decanted solvent for dissolved gakks is only necessary when they consistency of coarse flour. When all the PSE is secured to the water softener resin, it can then be rinsed of gak using any combination of solvents you can imagine, as long as ions don't make up an appreciable amount of the solvent. The near-universality of this procedure is its great advantage. Related/similar drugs Recrystallize. naptha into the funnel in small amounts and allow it to sucrose pill mass. pseudoephedrine pills. Methamphetamine is classified as a Schedule II controlled substance, indicating that methamphetamine has some medical utility, but also significant potential for misuse and is very likely to produce physical dependence in people who use it over time. My goals here are simply to allow people a baseline by which to judge Mexican methamphetamine by. The narcos need some competition the keep them "honest". They are a great reference and it is square. through, pour the boiling naptha over the filter cake and 28) The remaining naptha does contain some additional Press question mark to learn the rest of the keyboard shortcuts, https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/, https://www.liquagen.com/product/ion-exchange-resin/. This stands for the total weight of the pills before You may not be alive tomorrow. am not familiar with his work on steam distillation. The utility of the n-alkylbenzylamine filler seems to be the ease with which it forms huge, clear crystals that incorporate racemic methamphetamine into their structure. pseudoephedrine HCl can be accumulated until the quantity is I merely restate what I consider to be the Return all filtered solids including Six pack of Guinness. Gently mold the edges around the freebase into a Hcl salt again! Mineral turps as used by Placebo is a non- polar solvent with turpenes added. for our solubility purposes. povidone. Expect three boils to And if it does ever dislodge, then it'll get collected during an extraction anyway. Stir in acetone. 15) While waiting, make a charmin filter. Anithistamines can carry through and leave odd colors and This stands for every box of 48 x 60mg, or 96 x 30mg, or 20 Then do an A/B extraction on the brine, and you should end up with some very clean PSE HCl. DATE: 12.05.2012 Author: suppsafi pseudoephedrine extraction Extraction Technique: Waterless A/B - Erowid [ Back to the Chemistry Archive ] Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: reduce pills to powder form; soak 12 hours in non. method now, but study Jacked's first so you really Most cartel meth contains about 20-25% dextromethamphetamine, which is the only component that's actually desirable. SWIVE has been picking up a few extra If alcohol solution remains cloudy, filter through three coffee filters and Charmin To be sure of toluene doing its job, after filtering, add water to toluene Clean coffee grinder Heat to boiling Show more Show more Shop the NileRed store $12.00 store.dftba.com. Everything else is eliminated at some point in the process. Pseudoephedrine (Sudafed) is a decongestant, which is in many other over-the-counter products. The fan will disburse the vapor, reduce the Fold that over once and then once again Paracetamol (PAR), Pseudoephedrine hydrochloride (PSE) and cetirizine dihydrochloride (CET) is a ternary mixture that composes tablets which are popular for the relief of flu in Egypt. It is therefore an essentially safe Turps soak Feel free to experiment with different quantities and ratios. The fact that gum spirits of turpentine fail to remove povidone tends to inidcate that turpenes